Getting the data
The data are stored at the odin-server, please is accessible via the university network by choosing "map network drive" in the Windows file explorer, and connecting to "\\odin.nt.ntnu.no\xrd". Please email the lab responsible for getting access.the log-in details.
Analysing the data
Available software:
Name | Version | Publisher | Commonly used for | Useful links |
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Availability at NTNU4.2 analysisDescription: to come.0Modelling and fitting | | | | | | | | |
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Phase quantification |
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Vesta |
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How to install the software on own PC:
Open up an explorer window and go to the odin drive, as described above. Select the XRD_analysis_software folder. Double click on the relevant folder, and copy the relevant files to your computer, and start the installation (.exe) file.
Getting started
Topas : Example: Pawley fit of TiO2 (anatase and rutile) from Topas Workshop Hands-on tutorial no. 2: Topas Hands-on 2
Emission profiles:
For analysing XRD data in Topas, you will need to use a suitable emission profile (see for example here for explanation).
DaVinci1:
A while after the X-ray tube has been changed, some W contamination wavelengths will appear. Therefore we are regularly making new measurements from a LaB6 standard in order to have an up-to-date emission profile. This can be found on the odin-server, under "useful_documents\d8_davinci_1\Topas_Refinement_Details". Select the ".lam" file that has been made before your own measurements.
D8 Focus:
Here we are using a Ni-filter which removes the extra contamination wavelengths, such that we can use the pre-written emission profile "CuKa5.lam" that is included in the Topas installation directory ("C:\TOPAS5\Lam").
Plotting the data
Useful plotting software for XRD